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Melting Point

Panoramica

Source: Vy M. Dong and Jan Riedel, Department of Chemistry, University of California, Irvine, CA

One of the most important properties of a crystalline solid is its melting point. It can be used to determine the purity of a known compound and gives important information about the stability of the formed crystals.

Procedura

1. Sample Preparation

  1. Take a special glass capillary that fits the melting point apparatus in use.
  2. Dip the open end of the capillary into a sample of benzoic acid
  3. Gently tap the glass capillary on a hard surface, like a table, so that the benzoic acid moves down to the very bottom of the glass capillary

2. Measuring the Melting Point

  1. Insert the glass capillary into the melting point apparatus.
  2. Heat the apparatus with a rate of 10 

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Risultati

A sample of pure benzoic acid will melt at 122 °C.

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Tags

Melting PointSolidTemperatureOrganic CompoundsPurityIdentityMeasurementApplicationsSolid PhaseAmorphous SolidsCrystalline SolidsLattice StructureIntermolecular ForcesThermodynamic ConditionCoexistMelting RangeThermodynamic PropertyChemical Data

Vai a...

0:04

Overview

0:39

Principles of Melting Point

3:01

Melting Point Measurement Protocol

3:54

Applications

4:53

Summary

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